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Internal stresses and structure of multilayer coatings on the basis of Zr-Y-O / Si-Al-N

机译:基于Zr-Y-O / Si-Al-N的多层涂层的内应力和结构

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摘要

X-ray and TEM research of the structure of multilayered coatings consisting of the alternating layers Si-Al-N and Zr-Y-O of equal thickness are carried out. It is shown that the boundaries between different layers are sharp enough, and the chemical composition in each layer is homogeneous. The phase composition of the layers on the basis of Zr-Y-O contains basicallynanocrystalline ZrO2 and the layers on the basis of Si-Al-N contain Si3N4 amorphous phase. The internal field of stresses is determined by X-ray and TEM analyses. It is established that thecrystal lattice curvaturetorsion and the internal elastic stresses depend on the grain cross-section size of the Zr-Y-O layer.
机译:对厚度相等的交替层Si-Al-N和Zr-Y-O组成的多层涂层的结构进行了X射线和TEM研究。结果表明,不同层之间的边界足够尖锐,并且每一层中的化学成分均一。基于Zr-Y-O的层的相组成基本上包含纳米晶ZrO 2,并且基于Si-Al-N的层的相组成包含Si 3 N 4非晶相。内部应力场由X射线和TEM分析确定。可以确定的是,晶格弯曲和内部弹性应力取决于Zr-Y-O层的晶粒截面尺寸。

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